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Differential thermal analysis equipmentの製品一覧

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[Analysis Case] Pyrolysis GC/MS Double Shot Method, Identification of Plastics and Additives

[Analysis Case] Pyrolysis GC/MS Double Shot Method, Identification of Plastics and Additives

Composite analysis using TG-DTA and GC/MS.

By combining TG-DTA (thermogravimetric-differential thermal) analysis with GC/MS analysis, it is possible to select optimal temperature conditions to identify unknown polymer materials and the volatile organic compounds they contain. By investigating the pyrolysis temperature of the plastic parts of commercial products and continuously performing GC/MS measurements under two conditions—gentle heating below the pyrolysis temperature (thermal desorption method) and subsequent rapid heating at high temperatures (pyrolysis method) using the double-shot method—it was determined that this plastic is AS resin and contains the antioxidant additive IRGANOX 1076.

  • Contract Analysis
  • Differential thermal analysis equipment

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TG-DTA (Thermogravimetric Differential Thermal Analysis)

TG-DTA (Thermogravimetric Differential Thermal Analysis)

Output the temperature difference between the sample and the reference material as a DTA signal! Change the temperature according to a constant program.

TG-DTA (Thermogravimetric Differential Thermal Analysis) is an analysis that simultaneously measures the weight of a sample (TG) and the temperature difference between the sample and a reference material (Differential Thermal Measurement) (DTA) as a function of temperature, while varying the sample's temperature according to a specific program. The measurable conditions are a temperature range of room temperature to 1000°C, a required sample amount of 10 to 20 mg, and sample shapes including film, powder, and bulk. 【Features】 - Thermogravimetric Differential Thermal Analysis - Varies the sample's temperature according to a specific program - Simultaneously measures the sample's weight and the temperature difference from the reference material as a function of temperature - Required sample amount: 10 to 20 mg - Sample shapes include film, powder, and bulk *For more details, please refer to the PDF document or feel free to contact us.

  • Contract measurement
  • Contract Analysis
  • Contract Inspection
  • Differential thermal analysis equipment

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[Analysis Case] Quantification of water generated when heating water-absorbent polymers.

[Analysis Case] Quantification of water generated when heating water-absorbent polymers.

This article presents a case where water adhered to the surface of nylon 6, known as a water-absorbing polymer, and water generated during thermal decomposition were quantified separately.

The TG-MS (Thermogravimetric-Mass Spectrometry) method involves introducing gases generated during the TG-DTA (Thermogravimetric Differential Thermal Analysis) measurement of a sample online to a mass spectrometer (MS) for analysis. This technique allows for the acquisition of information regarding the thermal decomposition behavior of the sample, the types of gases generated, and the temperature ranges at which these gases are produced. Additionally, by creating a calibration curve using standard substances, it is possible to quantify the generated gases. [Analysis Sample] Nylon 6 (PA6) [Analysis Equipment] TG-DTA: Rigaku Thermo plus EVO2 GC-MS: Agilent 8890GC/5977B Inert Plus [Analysis Results] The TG-MS method allows for the quantification of water generated from the sample, separated by temperature. [Summary] Using the TG-MS method, it is possible to understand the amount of moisture adhering to the sample length and the amount of moisture generated during thermal decomposition.

  • Contract measurement
  • Differential thermal analysis equipment

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[TG-DTA, -MS] Thermogravimetric Differential Thermal Analysis, Differential Thermal Balance - Mass Analysis Method

[TG-DTA, -MS] Thermogravimetric Differential Thermal Analysis, Differential Thermal Balance - Mass Analysis Method

TG-DTA simultaneously evaluates weight changes caused by heating (TG) and thermal behavior of endothermic and exothermic reactions (DTA).

TG-DTA-MS continuously evaluates not only TG and DTA but also the volatile components (MS). - TG allows for the detection of weight changes on the order of percentage. - DTA provides insights into reactions such as pyrolysis, melting, sublimation, oxidation, combustion, and phase transitions. - MS enables the structural estimation of volatile components and decomposition products.

  • Contract Analysis
  • Contract measurement
  • Differential thermal analysis equipment

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